Overview

In this section, we present all the results of the experiments that served as important checkpoints. These include the validation of successful vector construction, the successful validation of PAL-TBH interactions by yeast one-hybrid assay color development, the successful phenotypic characterization of PAL-TBH overexpression plants, and the significant increase of flavonoid substances in PAL-TBH overexpression plants.

Successful cloning of CsTBH gene

The following are the results of our successful cloning of CsTBH gene with the help of TOPO vector. We verified the consistency of our cloned CsTBH gene with that in the cucumber genome database (http://cucurbitgenomics.org/) by both PCR and sequencing of a single colony of E. coli, indicating that the cucumber material we selected in the natural state did not undergo mutation.

Fig.1 Sequencing results of CsTBH gene clones

Fig. 2 PCR results of single colony of E. coli with CsTBH gene clone
Successful construction of yeast single heterozygous vectors and overexpression vectors
Colony PCR of E. coli single colony

In order to further study the gene function and explore the relationship between genes and genes, we need to construct different vectors to carry out our research, the following are the gel electrophoresis graphs obtained from the PCR of E. coli colonies and single colonies of overexpression of PCY, yeast monoheterozygous PJG and PLacZi vectors constructed by us, respectively, in which the red box, yellow box and blue box represent the length of the target fragments of PCY, PJG and PLacZi, respectively, and the length of the bands are consistent with our expectation. PLacZi, and the lengths of the target fragments shown by the bands were all consistent with our expectations.

Fig. 3 Growth of constructed E. coli colonies of TBH-PCY, PAL-PCY, PJG and PLacZi vectors on culture medium

Fig.4 Single colony PCR running gel bands of constructed TBH-PCY, PAL-PCY, PJG and PLacZi vectors for E. coli sequencing

We directly sequenced the single colonies picked from the plates coated after ligation transformation to verify whether they were consistent with the sequence of our target gene. Below are the graphs of the sequence results comparison.

Fig.5 Sequencing results of CsTBH-PCY vector

Fig.6 Sequencing results of CsPAL-PCY vector

Fig.7 Sequencing results of CsTBH-PJG vector

Fig.8 Sequencing results of CsPAL-LacZi vector
Yeast single hybridization test to verify the interaction between PAL and TBH

By observing our color development results, we found that the yeast round spots in the positive control group turned blue, the yeast round spots in the experimental group turned blue, while the yeast round spots in the negative control group did not undergo any color change, which proved that our selected CsTBH gene would bind with the downstream cis-acting regulatory element on the promoter of the CsPAL gene, and the two of them would interact.

Fig. 9 Yeast color development in chromatographic plates and analysis of interactions
The phenotype of overexpression plants was successfully identified

Observation of the overexpression plants showed that their cucumber fruits grew many small black spines compared with the wild type, which might be the key to the production of flavonoids, and further testing is needed to verify this.

Fig.10 Fruit phenotypes of CsTBH overexpressing transgenic plants
Determination of total human flavonoids by liquid chromatography mass spectrometry (LC-MS)

In order to clarify whether the fruits of CsTBH overexpression plants that we cultivated using gene editing could produce more flavonoids, by referring to the methods of some scientists [1], we quantified the flavonoid content within the wild-type and mutant fruits by using liquid chromatography mass spectrometry (LC-MS), and the following are the results of the assay, which are presented in the form of bar graphs.

Fig.11 Mass spectra and bar graphs of total flavonoids content in the fruits of CsTBH overexpression plants by LC-MS
References

[1] Feng Z, Sun L, Dong M, et al. Novel players in organogenesis and flavonoid biosynthesis in cucumber glandular trichomes. Plant Physiol. 2023;192(4):2723-2736. doi:10.1093/plphys/kiad236